A mixture of solids containing a ketone, a carboxylic acid, and an amine, are dissolved in DCM. What is the best way to begin an extraction to separate the amine from the mixture

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30-11-2021
Chemistry

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A mixture of solids containing a ketone, a carboxylic acid, and an amine, are dissolved in DCM. What is the best way to begin an extraction to separate the amine from the mixture

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Martebi Martebi · Answer 1 · 2021-12-08T13:21:46+01:00

There are different ways of extraction. The best way to begin an extraction to separate the amine from the mixture is to extract with dilute NaOH.

An acid-base extraction is often used in the extraction of carboxylic acids from the organic layer and thereafter into the aqueous layer.

NaOH is known to be the most common compound that is used to convert a carboxylic acid into its more water-soluble ionic carboxylate form.

But if the mixture has a compound that you want, and that can react with NaOH, another milder base such as sodium bicarbonate is preferably used.

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A mixture of solids containing a ketone, a carboxylic acid, and an amine, are dissolved in DCM. What is the best way to begin an extraction in order to separate the carboxylic acid from the mixture?

A) Extract with dilute NaOH

B) Extract with dilute HCl

C) Extract with dichloromethane

D) Extract with water

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